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High-power pulsed-laser--induced reactive quenching at liquid-solid interface is used for the first time to synthesize a metastable form of iron oxide. The oxide phase is characterized by using the techniques of conversion-electron M\"ossbauer spectroscopy, Rutherford backscattering spectrometry, x-ray diffraction, and x-ray photoelectron spectroscopy.
Patil et al. (Mon,) studied this question.