Experimental demonstration shows how interpenetration affects framework architecture, indicating design potential for 3D COFs.
isomerization, imparting pronounced framework flexibility and driving an exceptional ∼220% expansion of the crystal volume. This work provides the systematic experimental demonstration that interpenetration can be harnessed to govern both framework architecture and dynamic behavior, highlighting its key role in designing 3D COFs with tailored functions.
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Ye et al. (2026) studied this question.
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