Preparation and Characterization of Sol-gel Silica-modified Kenaf Bast Microfiber/Polypropylene Composites

The present study was conducted to determine the influence of the chemically modified kenaf bast fiber (KBF) on the mechanical, morphological, and thermal properties of fiber-reinforced polypropylene composites. The KBF was modified via the in situ sol-gel silica process through soaking the KBF in tetraethyl orthosilicate (TEOS) at a pH of 11, room temperature (25 °C ± 1 °C), and a KBF to TEOS ratio of 1:10 for 24 h. Silica successfully formed on the surface of the KBF. Subsequently, the sol-gel silica-modified KBF was utilized to produce sol-gel silica-modified KBF-reinforced polypropylene (PP-KBF-S) composites. Several analytical methods were utilized to determine the mechanical, morphological, and thermal properties of the PP-KBF-S composites, which were then compared with those of the untreated KBF-reinforced polypropylene composite. The findings revealed that sol-gel silica modification of the KBF reduced the void content and enhanced the mechanical properties and thermal stability of the PP-KBF-S.