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Palladium‐catalyzed telomerization of butadiene with O ‐acetylated pyranoses having a free anomeric hydroxyl group was applied for synthesis of octadienyl glycosides. The ratio of linear to branched glycosides depends dramatically on the conditions used. By careful optimization of reaction parameters the highly selective formation (95:5) of linear glycosides was achieved. An extended mechanism of the telomerization reaction is proposed. (© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2004)
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Hénin et al. (2004) studied this question.
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