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The unidentate trans-HNNH ligand in 1 (M = Os) is the most significant structural feature of this surprisingly stable compound. The positions of the two H atoms in the diazene were located and refined in the X-ray structural analysis. Compound 1 and the analogous Ru complex were prepared by the oxidation of the corresponding hydrazine complexes.
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Cheng et al. (1994) studied this question.
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