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The complementary informations from field desorption and electron impact mass spectra of free tripeptides and thyrotropine releasing hormone derivatives can be used to determine primary structure and molecular weight. Characteristic and diagnostic fragmentation pathways, the formation of diketopiperazines and the temperature-dependent tendency to form amine fragments and diketopiperazines will be discussed.
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Lüderwald et al. (1978) studied this question.
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