Overall rate constants for complex formation of Na + and Ca 2+ with antamanide and of Na + with perhydro‐antamanide were determined by using the temperature‐jump relaxation technique. Measurements were carried out in methanol or acetonitrile as solvents. Murexide was used as Na + ‐indicator. The reaction enthalpy of the Na + ‐antamanide system was determined from relaxation amplitudes. Values of the rate constants are considerably lower than those for similar macrocyclic complex‐forming compounds.
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Bürgermeister et al. (1974) studied this question.
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