A new approach to the study of the electrochemical oxidation of glucose in phosphate buffer is presented. The use of on‐line mass spectroscopy allows the direct analysis of production during a potential scan. Adsorbed intermediates are investigated by applying a flow cell technique in combination with mass spectroscopy in solutions containing ( 13 C) glucose. For comparison, the results for potassium gluconate are reported.
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Bolzán et al. (1987) studied this question.