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E.S.R. studies of KCl single crystals doped with small amounts of K3Ir(CN)6 and submitted to a prolonged 2 MeV electron irradiation at room temperature reveal the presence of the species [Ir(CN)5Cl]4- and [Ir(CN)4Cl2]4-. Ligand spin densities and ligand field parameters are calculated from the experimental hyperfine and superhyperfine interactions and compared with previous data on the species [Ir(CN)5]4-.
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Vugman et al. (1983) studied this question.
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