Experimental study demonstrates efficient electrochemical C–H arylation of five-membered heteroarenes using in situ diazotized anilines, suggesting a sustainable radical pathway for biaryl synthesis.
A simple and efficient electrochemical C–H arylation of five- membered active heteroarenes involves the application of arenediazonium salts generated in situ from anilines and tert - butyl nitrite. A cathodic reduction-induced radical chain mechanism is proposed.
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Liu et al. (2024) studied this question.
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