Polynuclear Cobalt Complexes. III. On meso ‐[(en) 2 Co(OH) 2 Co(en) 2 ] (NO 3 ) 4 The structure of the title compound has been determined by X‐ray analysis and refined to R = 0,060. The crystals are monoclinic, space group very probably C2/m, with cell dimensions a = 16,113(3), b = 10,946(2), c = 7,193(2) Å, β = 113,22(2)° and Z = 2. The configuration of the cation is ΔΛ IR. and UV./VIS. spectroscopic data are given.
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Thewalt et al. (1977) studied this question.
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