Electrochemical reaction demonstrates efficient synthesis of N-sulfonyl iminophosphoranes, suggesting a green method for phosphorus compounds.
An electrochemical P=N bond-forming reaction is demonstrated, which provides a practical and environmentally friendly method to access N-sulfonyl iminophosphoranes. This protocol exhibits broad substrate scope, good functional group tolerance, and good atom economy. Mechanistic studies, supported by cyclic voltammetry analysis, suggest that the reaction might begin with the anodic oxidation of trisubstituted phosphines.
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Yuan et al. (2026) studied this question.
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