A straightforward synthesis provides surprisingly stable, neutral and anionic μ3-imidorhodium clusters. The unusual complex [Rh4(μ-MeC6H4N)2(cod)4], whose structure is shown on the right, contains two bridging imido ligands that cap a triangle of metal atoms. One of these ligands, in addition, coordinates through the p-tolyl ring to a [Rh(cod)] moiety in a n5-cyclohexadienyl-like fashion. cod = 1,5-cyclooctadiene.
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Tejel et al. (1996) studied this question.
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