We report the syntheses, structures and magnetic properties of two decametallic Ni(II) clusters with unprecedented supertetrahedral cores, stabilised by the (hitherto unobserved) micro(6)-coordination modes of the tris-alkoxides [MeC(CH(2)O)(3)](3-) and [C(6)H(9)O(3)](3-).
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Shaw et al. (2004) studied this question.
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