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Potential cycling of a polypyrrole‐coated platinum electrode for several cycles between −1 and 0.5 V vs. in an aqueous 2,5‐dimercapto‐1,3,4‐thiadiazole, DMcT, solution induced a significant modification of the cyclic voltammogram. This modified cyclic voltammogram is still observed when the electrode is cycled in an electrolyte containing no added DMcT, suggesting that a new composite electrode material was being formed.
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Ye et al. (1994) studied this question.
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