Xenon was inserted into C(60) by heating C(60) in 3000 atm of xenon gas at 650 degrees C. The Xe@C(60) was separated from the empty C(60) by using HPLC. The (13)C resonance for Xe@C(60) is shifted downfield by 0.95 ppm (192 Hz). (129)Xe NMR showed a line 179.2 ppm downfield from xenon gas.
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Syamala et al. (2002) studied this question.
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