A new solution to an old problem: Remarkably regioselective de-O-benzylation of perbenzylated cyclodextrins (CDs) such as 1 (or α- and γ-CDs) occurs with diisobutylaluminum hydride, thus providing an innovative approach to the preparation of selectively modified cyclodextrins such as 2 in excellent yield.
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Pearce et al. (2000) studied this question.
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