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February 1, 1960Review of Scientific Instruments

Ultra-High-Pressure, High-Temperature Apparatus: the ``Belt''

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Authors

HHH. Tracy HallBrigham Young University

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Overview

Experimental study demonstrates sustained 100,000 atmospheres and 2000°C using a belted chamber apparatus, suggesting new avenues for ultra-high-pressure high-temperature synthesis.

Key Points

  • To develop and evaluate a stable apparatus capable of maintaining extreme pressures and high temperatures simultaneously over prolonged experimental durations.
  • Engineered an apparatus featuring opposed conical Carboloy pistons that push into a contoured Carboloy chamber, reinforced laterally with prestressed binding rings.
  • Fabricated composite sandwich gaskets utilizing naturally occurring pyrophyllite and a steel cone to achieve single-stage multistaging, pressure containment, and electrical and thermal insulation.
  • Implemented resistive sample heating via electric current passed through an internal metal or graphite tube alongside standardized temperature and pressure calibration procedures.
  • Maintained static pressures of 100,000 atmospheres concurrently with temperatures exceeding 2000°C for extended periods of time.
  • Achieved durable pressure sealing and axial piston travel without structural failure via the compressible pyrophyllite-steel gasket assembly.

Cite This Study

H. Tracy Hall (1960) studied this question.

synapsesocial.com/papers/6a7ce73c7394a4db165dfed2https://doi.org/10.1063/1.1716907
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