The electrochemical process involved in electrospray ionization is used to obtain odd-electron molecular ions from C(60)-TTF-C(60) and its methano derivatives. Exact mass measurements obtained using high-resolution mass spectrometry are reported, and the gas-phase behavior of the radical cation (retro-Diels-Alder reaction and [M/2 + H](+) ion formation) is described.
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Rondeau et al. (2001) studied this question.
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