A breath of fresh air: Air oxidation of [nBu4N]2[NiII(1-nor)3Br], prepared from [nBu4N]2[NiIIBr4] and 1-norbornyllithium generates the title pseudotetrahedral organometallic complex in which a nickel center with the formal oxidation state of +4 is present (see structure; Ni purple, Br brown, C black, H green).
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Dımıtrov et al. (2003) studied this question.
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