Indexed X-ray powder diffraction data are reported for the low temperature tetragonal ZrO 2 obtained by crystallization of zirconia gel. The structure was refined by the Rietveld technique on the basis of space group P 4 2 / nmc . Refined unit cell dimensions are a = 3.5984(5) Å, c = 5.152(1) Å, V = 66.71 Å 3 , D x =6.135 g / cm 3 , F 18 =62 (0.012, 24), R P =8.99, R wp =11.48, R B =3.13.
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Málek et al. (1997) studied this question.
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