Spectroscopic study demonstrates complete 1H and 13C NMR assignments for α- and β-d-glucofuranose, highlighting detailed structural parameters for minor sugar tautomers.
Although d-glucose is the most common sugar in nature, only a few NMR studies have focused on its minor furanose forms, and they have been limited to the anomeric position. Here, complete 1H and 13C NMR spectral analysis of α- and β-d-glucofuranose was performed, including signal assignment, chemical shifts, and coupling constants. Selective and non-selective 1D and 2D NMR experiments were used for the analysis, complemented by spin simulations and iterative spectral analysis.
No takes yet. Share an insight, caveat, or question.
Alexandersson et al. (2021) studied this question.
Synapse has enriched 5 closely related papers on similar clinical questions. Consider them for comparative context: