Experimental study demonstrates efficient dehydrative synthesis of dithiophosphinates via one-pot four-bond formation, suggesting a versatile approach for sulfur-phosphorus organic synthesis.
, and alcohols has been developed for the efficient dehydrative synthesis of dithiophosphinates. This method enables the one-pot construction of four chemical bonds (S-C-PS), delivering the target products with exclusive selectivity. A broad substrate scope, including a variety of allylic alcohols, benzyl alcohols, and even aliphatic alcohols, can be tolerated.
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Li et al. (2025) studied this question.
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