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Synthetic conditions of Pb-doped Bi-Sr-Ca-Cu-O oxide superconductors produced by a technique of a uniaxial hot-press method were studied. The quality of the samples was measured by means of X-ray diffraction analysis, secondary electron microscope measurement and density measurement. The hot-pressed sample showed a single 2223-phase with density close to the ideal value.
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Ikeda et al. (1990) studied this question.
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