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The Raman spectra of HSO 3 Cl in CH 3 COOH and NaSO 3 Cl in N,N ‐dimethylacetamide are recorded. From these spectra the SO 3 Cl − frequencies are reassigned. The new assignment is in agreement with the Raman spectra of solid (CH 3 ) 4 N · SO 3 Cl, SCl 4 · SO 3 , SeCl 4 · SO 3 and TeCl 4 · SO 3 .
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Stufkens et al. (1970) studied this question.
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