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The preparation and structural characterization of a series of lanthanide and uranium(IV) phthalocyanine halide complexes were achieved by reaction of the corresponding metal halide with Li 2 Pc. A preliminary survey of their reactivity includes ring reduction of Li(THF) 4 [PcUCl 3 ] with KC 8 leading to the first structurally characterized Pc 4− actinide complex, hydrolysis of PcDyCl(DMSO) to PcDyOH(H 2 O) 3 and preparation of a unique trimeric triangular Li(PcDy) 3 (OH) 4 (H 2 O) cluster.
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Zhou et al. (2020) studied this question.
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