The crystal structure of SbF 5 · SO 2 is reported. SbF 5 · SO 2 crystallizes in the monoclinic space group P2 1 /n with a = 580.4(4) pm, b = 1047.7(5) pm, c = 1013.3(6) pm, β = 102.92(5)°, V = 600.57 · 10 6 (6) pm 3 , and Z = 4. It shows five intermolecular S ··· F contacts.
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Minkwitz et al. (1989) studied this question.
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