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It is conclusively demonstrated using surface infrared spectroscopy, in combination with selective isotopic labeling, that methoxy coordinates with C₃ᵥ symmetry on Mo(110), at coverages below 0.17 ML. The existence of intense Fermi resonances in the C-H stretch region of adsorbed CH₃O is firmly established. By application of these observations to previous studies of methoxy on the low-index planes of copper and nickel, the disparity between the adsorbate geometry predicted by infrared spectroscopy and that deduced from photoelectron studies is removed.
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Uvdal et al. (1994) studied this question.
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