Magnesium-substituted birnessite and zinc chalcophanite have been synthesized through a novel procedure based on a combination of coprecipitation and metal ion intercalation techniques. The materials showed very promising performance as hosts for lithium intercalation. Upon galvanostatic discharge, Mg−birnessite and Zn−chalcophanite composite cathodes were able to intercalate >2 equiv of lithium per mole.
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Aronson et al. (1999) studied this question.
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