A new Li/Al layered double hydroxide, [LiAl 2 (OH) 6 ]Cl·2H 2 O, having a rhombohedral layer stacking sequence has been synthesized by the reaction of the Al(OH) 3 polymorphs, bayerite and nordstrandite, with LiCl. As is the case with the hexagonal analogue, rhombohedral [LiAl 2 (OH) 6 ]Cl·2H 2 O has been found to readily undergo anion exchange reactions with a range of dicarboxylate anions although these reactions differ significantly in that no crystalline staging intermediates could be isolated. The rhombohedral stacking is maintained in the dicarboxylate derivatives.
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Fogg et al. (2001) studied this question.
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