Summary: Three complementary techniques that probe different characteristics of curing: FTIR microspectroscopy, confocal microscopy and axisymmetric adhesion testing were used to study discrete epoxy samples cured at different temperatures and to follow curing across a continuous gradient combinatorial library. Together, these techniques provide a comprehensive picture of chemical and physical changes. FTIR microspectroscopy map of epoxy film cured on a temperature gradient. Red represents the highest and blue the lowest curing. magnified image FTIR microspectroscopy map of epoxy film cured on a temperature gradient. Red represents the highest and blue the lowest curing.
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Eidelman et al. (2004) studied this question.
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