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Experimental study demonstrates one-pot living radical polymerization and alkyne-azide click coupling using a single copper catalyst, highlighting streamlined functional polymer synthesis.
Azide terminally functional poly(methyl methacrylate)s (Mn = 4000-6000, PDI = 1.21-1.28) have been prepared by living radical polymerization and successfully reacted with alkynes in a Huisgen cycloaddition (click) reaction in one pot using the same catalyst for both processes.
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Mantovani et al. (2005) studied this question.
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