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A synthesis of an advanced intermediate towards the racemic form of the antiviral agent virantmycin has been developed featuring an intramolecular aza‐xylylene Diels–Alder reaction. The required arylthiocarbamate has been constructed using an efficient oxidative cyclization strategy. A novel synthetic approach to chlorine‐substituted allylic alcohols using an unprecedented palladium‐catalyzed cross‐coupling reaction of α,β‐unsaturated ketones and protected propargylic alcohols is reported.(© Wiley‐VCH Verlag GmbH & Co. KGaA, 69451 Weinheim, Germany, 2006)
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Keck et al. (2006) studied this question.
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