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Fluorophosphonium bromides are easily accessible by ligand exchange reactions between bromophosphonium bromides and difluorophosphoranes. The reaction between fluorophosphoranes of different Lewis acidity is investigated. Fluorophosphonium-organo-fluorophosphates are formed in some cases by transfer of fluoride ion. Alkylamino-substituted fluorophosphonium bromides may be obtained by Br/F-exchange in bromo-phosphonium bromides with sodium fluoride. The products are characterized by means of 1 H, 19 F, and 31 P NMR spectroscopy.
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Bartsch et al. (1981) studied this question.
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