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Reaction of trans-Mo(N2)2(syn-Me8[16]aneS4) with S8 gave trans-Mo(S)2(syn-Me8[16]aneS4) (1), which was also obtained by treating the N2 complex with t-BuSH through the C–S bond cleavage. The novel mononuclear structure of 1 was elucidated by an X-ray analysis.
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Yoshida et al. (1991) studied this question.
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