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Azidodifluoromethane was prepared in 65 % yield from chlorodifluoromethane by a two‐step synthesis using tributyl(difluoromethyl)ammonium chloride as an intermediate. The resulting azide was used in Huisgen azide‐alkyne reactions and ketone [3+2] cycloadditions to access novel N‐difluoromethyl‐1,2,3‐triazoles.
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Voltrová et al. (2018) studied this question.
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