The synthesis and crystal structure of 1-deoxy- d -lactose is described, as is its use as an additive in the crystallization of d -lactose. This has resulted in the formation of αβ- d -lactose for the first time at room temperature. Single-crystal analysis shows differences between this analysis and the structure previously obtained from powder data, particularly in the hydrogen-bonding patterns.
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Guiry et al. (2008) studied this question.
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