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The PE.‐spectra of triacetylene 1 (3), methyldiacetylene 2 (2), dimethylacetylene 3 (1) and dimethyldiacetylene 3 (2) have been recorded. The π‐ionization potentials of the unsubstituted acetylenes can be parametrized in terms of a LCBO‐model.
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Brogli et al. (1973) studied this question.
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