Watch your step! The individual steps during the chlorination of [Al13]− clusters via [Al11]−, [Al9]−, and [Al7]− intermediates (see picture) can be “visualized” by means of Fourier transform ion cyclotron resonance (FT-ICR) mass spectrometry. The reaction can be interpreted as a model reaction for the chlorination of bulk aluminum.
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Burgert et al. (2006) studied this question.
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