Construction by shining light! A [2+2] cycloaddition reaction in a 2D coordination polymer accompanied by single-crystal-to-single-crystal structural transformation to a 3D structure highlights the retrosynthesis of a 3D structure from a 2D layer compound (see scheme, Zn red, 4-styrylpyridine blue/turquoise).
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Medishetty et al. (2011) studied this question.
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