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Three luminescent palladium(II) and platinum(II) acetylide complexes, 1,3-[Cl(PEt 3 ) 2 PdC⋮CC 6 H 4 C⋮C] 2 -5-[( i Pr) 3 SiC⋮C]C 6 H 3 and 1,3,5-[Cl(PEt 3 ) 2 MC⋮CC 6 H 4 C⋮C] 3 C 6 H 3 (M = Pd or Pt), have been synthesized by the reaction of the corresponding starting complexes, trans -M(PEt 3 ) 2 Cl 2 (M = Pd or Pt), with branched alkynyl ligands. Their crystal structures, together with their luminescence behavior, have been reported.
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Yam et al. (2001) studied this question.
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