Summary Chloride in bucket milk samples from 100 cows was estimated by a modified Volhard method, an electrometric procedure, and direct titration with AgNO 3 . The readings of the electrometric procedure and the modified Volhard method were more closely related than those of the direct titration with AgNO 3 and the modified Volhard method. The electrometric procedure could be more readily conducted than the two other methods, and it practically eliminated operator variability in the detection of end points.
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Nageswararao et al. (1963) studied this question.