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Experimental study demonstrates metal-free catalytic hydroboration of multiple bonds in methanol under open air, suggesting a greener and accessible synthetic route.
An easy to operate method of catalytic hydroboration of unsaturated compounds has been developed with wide substrate scope. Reactions of various aldimines, ketimines, α,β-unsaturated carbonyl compounds, and alkynes were successfully executed with bis(pinacolato)diboron and N-heterocyclic carbenes in methanol without requiring a transition metal or inert atmosphere.
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Wen et al. (2013) studied this question.
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