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Propranolol is commonly assayed using the fluorimetric method reported by Shand, Nuckolls & Oates (1970).Other similar methods (Black, Duncan & Shanks, 1965, Potter, 1967, Lameijer, 1973) seem to be less accurate and practical, and they carry an additional toxicological risk because benzene is used as an extraction solvent.Recently the accuracy and sensitivity of the Shand et al. ( 1970) method has been criticized by Chidsey, Morselli, Bianchetti, Morganti, Leonetti & Zanchetti, (1975), because the g.l.c.method
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Offerhaus et al. (1976) studied this question.
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