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Alkylation of a tetrahedral cobalt(II)–dichloro complex bearing a sterically demanding and electron-donating diphosphine chelate gave a corresponding dialkyl-complex, which is the first coordinatively unsaturated cobalt(II)-(diphosphine)(dialkyl) complex isolated and characterized by X-ray analysis. This complex is expected to serve as a model intermediate in the cobalt(II)-catalyzed Heck-type reactions.
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Imamura et al. (2006) studied this question.
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