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In this communication, an unprecedented interception of CnF2n+1(O)SO. radical with a copper‐based carbene has been established. Distinguished by wide substrate scopes and mild reaction conditions, this novel radical–carbene coupling reaction (RCC reaction) provides a fundamentally different and mechanistically interesting strategy for the synthesis of perfluoroalkanesulfinate esters.
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Wang et al. (2018) studied this question.
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