We report on time resolved combined differential scanning calorimetry, small-angle and wide-angle x-ray scattering of hydrogen bonded flexible polymer-surfactant systems. The results show the presence of an order-disorder transition from a homogeneous to a lamellar structure due to dynamic coupling between surfactant and polymer. The homogeneous state exhibits a distinct small-angle x-ray scattering peak due to characteristic comb copolymerlike fluctuations. The peak position is strongly dependent on temperature and on the amount of surfactant material.
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Ruokolainen et al. (1996) studied this question.
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