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A new synthetic route leading to polysubstituted S-aryl sulfothioates, aromatic Bunte salts, is reported. Treatment of polysubstituted aromatic thiocyanates with sodium sulfite in aqueous DMF at room temperature affords polysubstituted S-(het)aryl sulfothioates. The novel transformation tolerates presence of a wide range of functional groups.
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Jansa et al. (2012) studied this question.
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