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a r b o n y l a t i o n r e a c t i o n s o f pentachloropyridine and 2,3,4,5-tetrachloropyridine were investigated in alcoholic or aqueous solvent.The high boiling alcohol 2-ethyl-1-hexanol was an effective carbonylation solvent above 100 o C at 1 atm of CO, representing a convenient and simple method for carrying out transition metal catalyzed carbonylation reactions using standard laboratory glassware.
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Hull et al. (2004) studied this question.
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