Styrene−methyl methacrylate−glycidyl methacrylate terpolymers to be used as binders in powder coating materials were synthesized in a homogeneous fluid phase containing 20 wt % CO 2 . Reactions carried out at 120 °C and 350 bar yield almost complete monomer conversion. The molecular weights were around 3000 g·mol -1 with a polydispersity index of 1.7. Molecular weight control was achieved by n -dodecyl mercaptan or by a catalytic chain-transfer agent. Simulations of the cumulative and differential copolymer composition are in excellent agreement with experimentally derived values.
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Beuermann et al. (2003) studied this question.
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